Fe3O4/MgO(100)薄膜的激光分子束外延与磁电学性能
Magnetic and electrical properties of Fe3O4/ thin films on MgO(100) substrates by laser molecular beam epitaxy
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摘要: 采用激光分子束外延方法，以烧结α-Fe2O3/为靶材，在MgO（100）基底上制备了Fe3O4薄膜。通过反射高能电子衍射原位观察了薄膜生长前后的表面结构，结果表明所生长的Fe3O4薄膜表面平整。经显微激光拉曼光谱和X光电子能谱分析证实所得薄膜表面成分为纯相Fe3O4。磁电学性能采用多功能物性系统测量，结果表明：当温度降至100 K附近时，薄膜电阻率有较大增加，Verwey相转变的范围变宽而且不明显，说明反向晶粒边界的存在；在7 160 kA·m-1的磁场下，室温磁电阻达到-6.9%，在80和150 K温度下磁电阻分别达到-10.5%和-16.1%；薄膜的室温饱和磁化强度约为260 kA·m-1，其矫顽磁场约为202 kA·m-1。Abstract: Using sintered α-FeFe2O3 as target, FeFe3O4 thin films were grown on MgO (100) substrates by laser molecular beam epitaxy. The quality of the films was checked in situ by monitoring reflection high energy electron diffraction patterns during deposition. The results showed that the surface of the films is smooth. Raman spectroscopy and X-ray photoelectron spectroscopy(XPS) analysis confirms the presence of single-phase FeFe3O4 in the surface of the films, and no other iron oxides exist. The magnetic and electrical properties of the FeFe3O4 thin films were investigated. The results showed that the resistivity of the Fe3O4 thin films increases sharply about 100 K, and the temperature range of Verwey trans
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Key words:
- thin films /
- half-metal /
- laser molecular beam /
- epitaxy /
- coercivity
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