Volume 25 Issue 08
Nov.  2013
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Chen Bowei, Bi Yutie, Luo Xuan, et al. Microstructure of zinc-based composite aerogels[J]. High Power Laser and Particle Beams, 2013, 25: 1984-1988. doi: 10.3788/HPLPB20132508.1984
Citation: Chen Bowei, Bi Yutie, Luo Xuan, et al. Microstructure of zinc-based composite aerogels[J]. High Power Laser and Particle Beams, 2013, 25: 1984-1988. doi: 10.3788/HPLPB20132508.1984

Microstructure of zinc-based composite aerogels

doi: 10.3788/HPLPB20132508.1984
  • Received Date: 2012-10-08
  • Rev Recd Date: 2013-03-12
  • Publish Date: 2013-06-19
  • The zinc-based composite aerogel was prepared by the sol-gel method using ZnCl2 as precursor, polyacrylic acid (800, 1800, 5000) as template, and propylene oxide as initiator. The characterization of aerogels was carried out by field-emission scanning electron microscope (FESEM), high-resolution transmission electron microscopy (HRTEM), and N2 adsorption/desorption. The results suggested that the zinc-based composite aerogel made by polyacrylic acid (1800) had perfectly three-dimensional networks and the skeletal was composed of particles in nanometer and had a high surface area about 236 m2/g. The N2 adsorption/desorption showed the aerogel had an average pore-diameter of 11 nm and a total pore volume of 0.179 cm3/g.
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