Preparation of poly(imine imine ketone)s microshells

cui yi; luo xuan; fan yongheng; liu lei; lin runxiong; zhang lin

Volume 22 Issue 12

Dec. 2010

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cui yi, luo xuan, fan yongheng, et al. Preparation of poly(imine imine ketone)s microshells[J]. High Power Laser and Particle Beams, 2010, 22.

Citation:

cui yi, luo xuan, fan yongheng, et al. Preparation of poly(imine imine ketone)s microshells[J]. High Power Laser and Particle Beams, 2010, 22.

cui yi, luo xuan, fan yongheng, et al. Preparation of poly(imine imine ketone)s microshells[J]. High Power Laser and Particle Beams, 2010, 22.

Citation:

cui yi, luo xuan, fan yongheng, et al. Preparation of poly(imine imine ketone)s microshells[J]. High Power Laser and Particle Beams, 2010, 22.

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Preparation of poly(imine imine ketone)s microshells

1.
Engineering Research Center of High Performance Polymer and Molding Technology,Ministry of Education,Qingdao University of Science and Technology,Qingdao 266042,China;
2.
Research Center of Laser Fusion,CAEP,P.O.Box 919-987,Mianyang 621900,China

Publish Date: 2010-12-07

Abstract

Abstract

Large diameter (0.6～2.0 mm) microshells of poly (imine imine ketone)s (PIIKs) were prepared by microliquid technique and doublelayer latex technique. A double T-channel droplet generator was designed and developed for the fabrication of PIIKs microshells of controlled size continuously. Manipulative conditions of the diameter and thickness of shells were studied, and the effect of density mismatch on shell quality was discussed. Phase separation during the preparation process affects the morphology of shells. Spinodal phase separation tends to occur at the outer surface of the shells，while binodal phase separation at the inner surface. The diameters of PIIKs shells were measured, 88% of which vary in ±5% of the average diameter. The sphericity is better than 99%．
- micro-liquic,
- micro-shells,
- piiks,
- monodispersity

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