Volume 16 Issue 02
Feb.  2004
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zu xiao-tao, feng xiang dong, zhang chuan-fei, et al. Effect of isothermal annealing on microstructure of irradiation-induced amorphous TiNiCu alloys[J]. High Power Laser and Particle Beams, 2004, 16.
Citation: zu xiao-tao, feng xiang dong, zhang chuan-fei, et al. Effect of isothermal annealing on microstructure of irradiation-induced amorphous TiNiCu alloys[J]. High Power Laser and Particle Beams, 2004, 16.

Effect of isothermal annealing on microstructure of irradiation-induced amorphous TiNiCu alloys

  • Publish Date: 2004-02-15
  • Recrystallization of irradiationinduced amorphous TiNiCu alloys has been investigated by means of the in situ transmission electron microscopy (TEM). TiNiCu shape memory alloy samples were amorphized by 400keV Xe+ ions at room temperature using IVEMTandem Facility at Argonne National Laboratory. The recovery process of amorphization was observed upon annealing from room temperature to 750℃ at a rate of 10℃ /min by in situ TEM. The recrystallization started when annealing at 280℃ for 10 min and the diffraction spots appeared around the amorphous rings. The polycrystalline rings started to form at 550℃ and the recrystallization basically finished at 750℃. The polycrystalline rings are indexed to TiNiCu SMAs. The microstructure after the recrystallization is different from that of th
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